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02 Feb #5 If he made use of acidification with drinking water and DCM, then he separated drinking water layer with four-MMC*HCl and afterwards washed this layer with DCM many situations. After that you can depart it in container for crystallization. Just my ideas. May be various from his process.
3-MMC incorporates a chiral heart about the C-two carbon. Subsequently two enantiomers exist, the R and S enantiomer. It’s assumed the S variety is much better because of its similarity to cathinone. Nonetheless added exploration needs to be performed to validate this.